ASAP2050 Operator's Manual

ASAP 2050

Extended Pressure Adsorption Analyzer

Operator’s Manual

V1.01

205-42801-01

May 2010

Kalrez is a registered trademark of DuPont Dow Elastomers L.L.C.

Teflon is a registered trademark of E.I. DuPont de Nemours Company

Windows is a registered trademark of Microsoft Corporation

Fomblin is a registered trademark of Ausimont

? Micromeritics Instrument Corporation 2007-2010. All rights reserved.

The software described in this manual is furnished under a license agreement and may be used or copied only in accordance with the terms of the agreement.

WARRANTY

MICROMERITICS INSTRUMENT CORPORATION warrants for one year from the date of shipment each instrument it manufactures to be free from defects in material and workmanship impairing its usefulness under normal use and service conditions except as noted herein.

Our liability under this warranty is limited to repair, servicing and adjustment, free of charge at our plant, of any instrument or defective parts when returned prepaid to us and which our examination discloses to have been defective. The purchaser is responsible for all transportation charges involving the shipment of materials for war-ranty repairs. Failure of any instrument or product due to operator error, improper installation, unauthorized repair or alteration, failure of utilities, or environmental contamination will not constitute a warranty claim. The materials of construction used in MICROMERITICS instruments and other products were chosen after extensive testing and experience for their reliability and durability. However, these materials cannot be totally guaranteed against wear and/or decomposition by chemical action (corrosion) as a result of normal use.

Repair parts are warranted to be free from defects in material and workmanship for 90 days from the date of shipment.

No instrument or product shall be returned to MICROMERITICS prior to notification of alleged defect and authorization to return the instrument or product. All repairs or replacements are made subject to factory inspec-tion of returned parts.

MICROMERITICS shall be released from all obligations under its warranty in the event repairs or modifications are made by persons other than its own authorized service personnel unless such work is authorized in writing by MICROMERITICS.

The obligations of this warranty will be limited under the following conditions:

1.Certain products sold by MICROMERITICS are the products of reputable manufacturers, sold under their

respective brand names or trade names. We, therefore, make no express or implied warranty as to such prod-ucts. We shall use our best efforts to obtain from the manufacturer, in accordance with his customary prac-tice, the repair or replacement of such of his products that may prove defective in workmanship or materials.

Service charges made by such manufacturer are the responsibility of the ultimate purchaser. This states our entire liability in respect to such products, except as an authorized person of MICROMERITICS may other-wise agree to in writing.

2.If an instrument or product is found defective during the warranty period, replacement parts may, at the dis-

cretion of MICROMERITICS, be sent to be installed by the purchaser, e.g., printed circuit boards, check valves, seals, etc.

3.Expendable items, e.g., sample tubes, detector source lamps, indicator lamps, fuses, valve plugs (rotor) and

stems, seals and O-rings, ferrules, etc., are excluded from this warranty except for manufacturing defects.

Such items which perform satisfactorily during the first 45 days after the date of shipment are assumed to be free of manufacturing defects.

Purchaser agrees to hold MICROMERITICS harmless from any patent infringement action brought against MICROMERITICS if, at the request of the purchaser, MICROMERITICS modifies a standard product or manu-factures a special product to the purchaser’s specifications.

MICROMERITICS shall not be liable for consequential or other type damages resulting from the use of any of its products other than the liability stated above. This warranty is in lieu of all other warranties, express or implied, including, but not limited to, the implied warranties of merchantability or fitness for use.

4356 Communications Drive Norcross, GA 30093-1877 Fax (770) 662-3696 Domestic Sales - (770) 662-3633 Domestic Repair Service - (770) 662-3666 International Sales - (770) 662-3660 Customer Service - (770) 662-3636

Form No. 008-42104-00

Rev. 12/95

TABLE OF CONTENTS

1.GENERAL INFORMATION

Organization of the Manual. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-1 Conventions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-3 Online Manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-4 Using Bookmarks. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-4

Using the Table of Contents, Index, and other Links. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-6 Table of Contents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-6

Index. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-7

Cross References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-7 Using the Find Command . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-8

Printing. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-9 Internet Access. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-10 Equipment Description. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-11 Gas Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-12 Analysis Program. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-12 Report System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-12 Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-13 b18bdb32eefdc8d376ee32b0ER INTERFACE

Controls, Indicators, and Connectors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1 Front Panel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1

Side Panel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-4 Upper . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-4

Lower . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-5 Rear Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-6

Turning On the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-6

Turning Off the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-6 Using the Software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-7 Shortcut Menus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-7

Shortcut Keys. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-7

Dialog Boxes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-9

Selecting Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-11 File Name Conventions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-13 Menu Structure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-14 Windows Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-15 Help Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-15 3.OPERATIONAL PROCEDURES

Sample Information Files. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-1 Specifying Sample File Defaults . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-2 Basic Format . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-2

Advanced Format. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-4 Creating Sample Information Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3-6

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