氟替卡松丙酸酯 [CAS80474-14-2]合成路线图解——原料药厂家东康源(4)

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List of intermediates

benzyl (2s)-6-azido-2-(1,3-dioxo-1,3-dihydro-2h-isoindol-2-yl)-6-methylheptanoate

(3s)-3-amino-7,7-dimethyl-2-azepanone

tert-butyl (3s)-7,7-dimethyl-2-oxoazepanylcarbamate

methyl 2-[(6s)-6-amino-2,2-dimethyl-7-oxoazepanyl]acetate

1-(2-bromoethoxy)-1-methylethyl 2-bromoethyl ether No. (i) (iii) (iv) (ii) (v)

Reference 1:

phillips, g.h.; bain, b.m.; williamson, c.; steeples, i.p.; laing, s.b. (glaxo wellcome plc); androstane 17beta-carbothioates. gb 2088877; nl 8100707; us 4335121 .

Reference 2:

phillips, g.h.; bailey, e.j.; bain, b.m.; et al.; synthesis and structure-activity relationships in a series of antiinflammatory corticosteroid analogues, halomethyl androstane-17beta-carbothioates and -17beta-carboselenoates. j med chem 1994, 37, 22, 3717.

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