氟替卡松丙酸酯 [CAS80474-14-2]合成路线图解——原料药厂家东康源(2)

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List of intermediates

benzyl (2s)-2-(1,3-dioxo-1,3-dihydro-2h-isoindol-2-yl)-6-hydroxy-6-methylheptanoate

benzyl (2s)-6-azido-2-(1,3-dioxo-1,3-dihydro-2h-isoindol-2-yl)-6-methylheptanoate

2-[(3s)-7,7-dimethyl-2-oxoazepanyl]-1h-isoindole-1,3(2h)-dione

(3s)-3-amino-7,7-dimethyl-2-azepanone

tert-butyl (3s)-7,7-dimethyl-2-oxoazepanylcarbamate No. (i) (ii) (iii) (iv) (v)

Reference 1:

edwards, j.a. (syntex (usa), inc.); 17beta-thiocarboxylic acid esters of 6alpha,6beta-difl

uoro-3-oxoandrost-4-enes. us 4187301 .

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