氟替卡松丙酸酯 [CAS80474-14-2]合成路线图解——原料药厂家东康源(6)

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List of intermediates

benzyl (2s)-2-(1,3-dioxo-1,3-dihydro-2h-isoindol-2-yl)-6-hydroxy-6-methylheptanoate

benzyl (2s)-6-azido-2-(1,3-dioxo-1,3-dihydro-2h-isoindol-2-yl)-6-methylheptanoate

2-[(3s)-7,7-dimethyl-2-oxoazepanyl]-1h-isoindole-1,3(2h)-dione

(2r,4r,5r,6r,8s,11s,12r,19r,20r)-5-[[(2s,3r,4s,6r)-4-(dimethylamino)-3-hydroxy-6-methyltetrahydro-2h-pyran-2-yl]oxy]-11-ethyl-4-methoxy-2,4,6,8,12,19-hexamethyl-13-oxa-15,18-diazatricyclo[10.6.2.0(15,20)]icos-1(18)-ene-7,9,14-trione No. (i) (ii) (iv) (iii)

Reference 1:

cooper, a.j.; chamberlin, s.a.; hufnagel, j.j.; barkalow, j.; hossain, a.; langridge, d.c. (abbott labo ratories inc.); method for the preparation of fluticasone and related 17betaeta-carbothioic esters using a novel carbothioic acid synthesis and novel purification methods. wo 0162722 .

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